Mac Tempas Manual
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Hi,
You may add to the in-situ experiment list some work we did here:
Work from M. Flueli thesis
HREM dynamic observation of gold nanocrystals (same as J.O. Bovin, D. Smith,..)
HREM dynamic observation of sintering of gold nanocrystals induced at room
temperature by the electron beam (M. Flueli et al., Surf. Sci. 202 (1988)
343-353)
Work from D. Ugarte
HREM in situ transformation of fullerenes into bucky onions (MRS Bull. XIX
no 11 nov. 1994,39-42; Europhys. Lett. 22 (1993) 45-50
If there is some interest, I can provide a video movie (about 10 min. at
total for these 3 items, at present with the european PAL standard, but
NTSC may be available too).
B. Hall and D. Reinhart do electron diffraction of silver clusters
produced in a supersonic He or Ar stream. They showed the co-existence in
various concentrations of fcc cuboctaheras, decahedras and icosahedras.
(B.D. Hall et al, Phys. Rev. B43 (1991) 3906-.., B.D. Hall et al., Rev.
Sci. Instrum. 62 (1991) 1481-1488, B.D. Hall et al., Z. Phys. D20 (1991)
457-.. and D26 (1993) S73-..)
There are also two others teams using in-situ in Lausanne (conventional
TEM). One (R. Gotthardt) in the field of in-situ straining of metals at
room, low or high temperature. The second one (G. Gagnon) has a video movie
of thermal fatigue, up to crack generation, for an Al based alloy
reinforced by oxides particles. I don't have the details right now. If
these authors have not answered to your call themselves, I am ready to find
more if anybody is interested.
Yours
__________________________________________________________________
Philippe Buffat Ecole Polytechnique Federale de
Lausanne (EPFL)
Centre Interdepartemental
de Microscopie Electronique
Address: EPFL-CIME, Batiment MX-C, CH-1015 Lausanne, Switzerland
Phone: +41(21)693 29 83 Fax: +41(21)693 44 01 (Central European Time)
E-mail: philippe.buffat-at-cime.uhd.epfl.ch // pabuffat-at-cimesg1.epfl.ch
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